Tips and coupons

Hardness readings for four tips on four metal coupons are

Tip 1 Tip 2 Tip 3 Tip 4
Coupon 1 9.3 9.4 9.2 9.7
Coupon 2 9.4 9.3 9.4 9.6
Coupon 3 9.6 9.8 9.5 10.0
Coupon 4 10.0 9.9 9.7 10.2

Treat coupons as blocks and tips as treatments in a randomised block design, with one observation per cell. Compute the two F statistics and state the conclusion of each test at level 0.05. The 0.95 quantile of F_{3,9} is about 3.86.

The grand mean of the 16 readings is 9.625. The tip means, the column means, are 9.575, 9.600, 9.450 and 9.875, so

\mathrm{SS}_{\mathrm{tip}}=4\sum_j(\overline y_{\cdot j}-9.625)^2=0.385, \qquad \mathrm{MS}_{\mathrm{tip}}=0.385/3=0.1283.

The coupon means, the row means, are 9.400, 9.425, 9.725 and 9.950, and \mathrm{SS}_{\mathrm{coupon}}=0.825, so \mathrm{MS}_{\mathrm{coupon}}=0.275. The total sum of squares is 1.290, so the error sum of squares is 1.290-0.385-0.825=0.080, on (4-1)(4-1)=9 degrees of freedom, and \mathrm{MS}_{\mathrm{error}}=0.008889.

F_{\mathrm{tip}}=\frac{0.1283}{0.008889}\approx 14.44, \qquad F_{\mathrm{coupon}}=\frac{0.275}{0.008889}\approx 30.94.

Both exceed 3.86. At level 0.05 the test rejects equal tip means, and the coupons also differ, which shows that blocking on the coupon removed a large source of variation from the error.